HCID 66795326, compound → HCID 19842620, compound

HRID 1532920Notes

Reaction equation

HRID 1532920 reaction equation
C[C@@:2]12[C@@H:10](O)[CH2:9]C[C@H:7]1[C@@H:6]1CCC3C=C(O)C=CC=3[C@H:5]1[CH2:4][CH2:3]2.[CH3:21][C@@:22]12[C@@H:38](O)[CH2:37]C[C@H:35]1[C@H:34]1[C@@H:25](C3C=CC(O)=CC=3CC1)[CH2:24][CH2:23]2>C(OCC)(=O)C>[CH2:9]=[CH:10][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:24]=[CH:23][C:22](=[CH2:21])[CH3:35].[CH2:37]=[CH:38][C:22]1[CH:35]=[CH:34][CH:25]=[CH:24][CH:23]=1

Participants

3

Reactant 1

HCID 66795326HCID 66795326, compound

Product 1

HCID 19842620HCID 19842620, compoundYield 26,277.6%

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

In a separate operation, a solution of 20 g hydrogenated colophony glycerol ester resin (Staybelite Ester® 5E) and 8 g styrene-isoprene-styrene copolymer (Cariflex® TR 1107) is prepared in 10 g ethyl acetate and 10 g naphtha having a boiling range between 80 and 100° C.; 0.12 g 17-β-estradiol is added which dissolves completely at room temperature. Using a gap width of about 100 μm, the mass is coated on an antiadhesive polyester film such that a uniform layer having a weight per unit area of 23 g/m2 results after drying for 30 minutes at 35° C. and afterdrying for 15 minutes at 60° C.

Workup

  1. dissolutiondissolves completely at room temperature
  2. customresults
  3. customafter drying for 30 minutes at 35° C.
  4. customfor 15 minutes
  5. customat 60° C.

Sources & evidence

ORD record
ord-f2deabee762649d9abfa70a86a937988
Source dataset
uspto-grants-2001_03
Patent number
US06207183B1

Reaction notes

Loading…