HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-(2-hydroxyphenyl)prop-2-enoate → Methyl 3-(2-hydroxyphenyl)propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-(2-hydroxyphenyl)prop-2-enoate | HCID 89400 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 3-(2-hydroxyphenyl)propionate | HCID 2794569 | 100.1% |
Reaction Steps
A mixture of methyl 3-(2-hydroxyphenyl)acrylate (2.47 g) and 10% palladium on carbon (0.50 g) in methanol (30 ml) was stirred under hydrogen atmosphere for 3 hours. The mixture was filtered and the filtrate was evaporated under reduced pressure to afford methyl 3-(2-hydroxyphenyl)propionate (2.50 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06207686B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-c4df573437c7492cb725e0551538753d |
| Source note | uspto-grants-2001_03 |