HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → HCID 12227892, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | 3-Fluoroaniline | HCID 9742 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Bis(2-chloroethyl)amine hydrochloride | HCID 522769 | — |
| Solvent | HCID 86745446 | HCID 86745446 | — |
| Product | HCID 12227892 | HCID 12227892 | 35.9% |
Reaction Steps
This compound was prepared according to the procedure of Preparation 1. A mixture of 8.0 g (0.045 mol) of bis(2-chloroethyl)amine hydrochloride, 5.0 g (0.045 mol) of m-fluoroaniline and 12.5 g (0.09 mol) of solid potassium carbonate in a total volume of 50 mL of n-butanol gave 3.5 g (35%) of white solid, mp 205°-207° C. (methanol-water-ethyl ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05086055 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-6db1d895c8d54ee7b58a5475cbb53e94 |
| Source note | uspto-grants-1992_02 |