HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 15030095, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 1-(2-Pyridyl)piperazine | HCID 94459 | — |
| Reactant | 5-(2-Chloro-ethyl)-3-methyl-oxazolidin-2-one | HCID 14698746 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 15030095 | HCID 15030095 | 75.8% |
Reaction Steps
This compound was prepared according to the procedure of Example 2. A mixture of 4.1 g (0.025 mol) of 1-(2-pyridinyl)piperazine, 4.1 g (0.025 mol) of 5-(2-chloroethyl)-3-methyl-2-oxazolidinone, 8.0 g (0.075 mol) of anhydrous sodium carbonate and 0.4 g of potassium iodide in 150 mL of 1-butanol gave 5.5 g (75%) of white solid, mp 107.5°-109° C. (2-propanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05086055 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-5a2f0499479e4b82b6011f132ad902e4 |
| Source note | uspto-grants-1992_02 |