HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 15030076, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 1-(4-Nitrophenyl)piperazine | HCID 80447 | — |
| Reactant | 5-(2-Chloro-ethyl)-3-methyl-oxazolidin-2-one | HCID 14698746 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 15030076 | HCID 15030076 | 79.3% |
Reaction Steps
This compound was prepared according to the procedure of Example 2. A mixture of 4.1 g (0.02 mol) of 1-(4-nitrophenyl)piperazine, 3.3 g (0.02 mol) of 5-(2-chloroethyl)-3-methyl-2-oxazolidinone, 6.4 g (0.06 mol) of anhydrous sodium carbonate and 0.4 g of potassium iodide in 100 mL of 1-butanol gave 5.3 g (79%) of yellow solid, mp 155°-156° C. (acetonitrile).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05086055 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-7067e05d5d244dc88bc11fe6bafa5648 |
| Source note | uspto-grants-1992_02 |