HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 15030081, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 1-(m-Tolyl)piperazine | HCID 83111 | — |
| Reactant | 5-(2-Chloro-ethyl)-3-methyl-oxazolidin-2-one | HCID 14698746 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 15030081 | HCID 15030081 | 65% |
Reaction Steps
This compound was prepared according to the procedure of Example 2. A mixture of 3.5 g (0.02 mol) of 1-(3-methylphenyl)piperazine (Emka-Chemie), 3.3 g (0.02 mol) of 5-(2-chloroethyl)-3-methyl-2-oxazolidinone, 6.4 g (0.06 mol) of anhydrous sodium carbonate and 0.4 g potassium iodide in 100 mL of 1-butanol gave 3.9 g (65%) of white solid, mp 72°-74° C. (2-propanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05086055 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-02fdb174883c4bef87d65385bf36076e |
| Source note | uspto-grants-1992_02 |