HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → HCID 15030085, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | 1-(2-Methoxyphenyl)piperazine | HCID 1346 | — |
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 86745448 | HCID 86745448 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 15030085 | HCID 15030085 | 63% |
Reaction Steps
This compound was prepared according to the procedure of Example 2. A mixture of 2.9 g (0.015 mol) of 1-(2-methoxyphenyl)piperazine (95%, Aldrich), 2.5 g (0.015 mol) of 5-(2-chloroethyl-3-methyl-2-oxazolidinone, 5.3 g (0.05 mol) of anhydrous sodium carbonate and 0.4 g of potassium iodide in 100 mL of 1-butanol gave 3.0 g (63%) of off-white solid, mp 107°-108.5° C. (2-propanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05086055 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-8356909ddc0c4b6784516a36328200c1 |
| Source note | uspto-grants-1992_02 |