Tert-Butylamine → HCID 14880461, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 7.75 g of the product of Step E, 6.83 g of potassium carbonate, 25.8 ml of tertbutylamine and 150 ml of ethanol was heated at 140° C. for 48 hours in an autoclave. After filtering, the filtrate was brought to dryness under reduced pressure and the 11.7 g of residue were chromatographed of silica (eluant: ethyl acetate-triethylamine (95-5)) to obtain 6.32 g of the desired product.

Provenance & Evidence