HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic Acid → Methanone, (2-(3-((1,1-dimethylethyl)amino)propoxy)phenyl)-1H-indol-4-yl-, monobenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic Acid | HCID 243 | — |
| Reactant | HCID 3077190 | HCID 3077190 | — |
| Product | Methanone, (2-(3-((1,1-dimethylethyl)amino)propoxy)phenyl)-1H-indol-4-yl-, monobenzoate | HCID 3077189 | 84.5% |
Reaction Steps
Using the procedure of Step G of Example 1, 3.0 g of the product of Step F, 1.05 g of benzoic acid were reacted to obtain 3.42 g of the product melting at 162° C., which was crystallized from isopropanol to obtain 2.73 g of the desired pure product melting at 162° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05086070 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-8c41d348e2634db4b408a4a48a463a59 |
| Source note | uspto-grants-1992_02 |