Benzoic Acid → HCID 54158777, compound

HRID 1533984Notes

Reaction equation

HRID 1533984 reaction equation
[CH3:1][C:2]([NH:5][CH2:6][CH:7]([OH:26])[CH2:8][O:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[CH2:16][C:17]1[CH:25]=[CH:24][CH:23]=[C:22]2[C:18]=1[CH:19]=[CH:20][NH:21]2)([CH3:4])[CH3:3].[C:27](O)(=[O:34])[C:28]1[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1>>[C:27]([O:26][CH:7]([CH2:8][O:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[CH2:16][C:17]1[CH:25]=[CH:24][CH:23]=[C:22]2[C:18]=1[CH:19]=[CH:20][NH:21]2)[CH2:6][NH:5][C:2]([CH3:1])([CH3:3])[CH3:4])(=[O:34])[C:28]1[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1

Participants

3

Reactant 2

HCID 243Benzoic AcidHCID 3077192HCID 3077192, compound

Product 1

HCID 54158777HCID 54158777, compoundYield 39.3%

Procedure

Using the procedure of Step G of Example 3, 16.3 g of the product of Step C and 5.65 g of the benzoic acid were reacted to obtain 8.29 g of the desired product melting at 195° C. (ethanol).

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-8d20334bf015471a98851b5fbd0635a1
Source dataset
uspto-grants-1992_02
Patent number
US05086070

Reaction notes

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