Benzoic Acid → HCID 14880478, compound

HRID 1533985Notes

Reaction equation

HRID 1533985 reaction equation
[CH3:1][C:2]([NH:5][CH2:6][CH2:7][CH2:8][O:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[CH2:16][C:17]1[CH:25]=[CH:24][CH:23]=[C:22]2[C:18]=1[CH:19]=[CH:20][NH:21]2)([CH3:4])[CH3:3].[C:26]([OH:34])(=[O:33])[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1>>[C:26]([OH:34])(=[O:33])[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1.[CH3:4][C:2]([NH:5][CH2:6][CH2:7][CH2:8][O:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[CH2:16][C:17]1[CH:25]=[CH:24][CH:23]=[C:22]2[C:18]=1[CH:19]=[CH:20][NH:21]2)([CH3:1])[CH3:3]

Participants

3

Reactant 2

HCID 243Benzoic AcidHCID 14880477HCID 14880477, compound

Product 1

HCID 14880478HCID 14880478, compoundYield 67%

Procedure

Using the procedure of Step G of Example 3, 8.12 g of the product of Step B and 2.95 g of benzoic acid were reacted to obtain 7.42 g of the desired product melting at 183° C. after crystallization from ethanol.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-89980d7d9867423ca24070e6d7f7bae2
Source dataset
uspto-grants-1992_02
Patent number
US05086070

Reaction notes

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