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HRID1533990

反应详情

EQUATION

反应方程式

HRID 1533990 的结构方程式

REACTANTS

反应物

2
结构：[O]=[Cr](=[O])([O-])[O][Cr](=[O])(=[O])[O-].c1cc[nH+]cc1.c1cc[nH+]cc1
HCID2724130

Chromic acid (H2Cr2O7), compd. with pyridine (1:2)

C10H12Cr2N2O7

结构：COc1ccccc1C(O)c1cccc2c1ccn2C
HCID19800111

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccccc1C(=O)c1cccc2c1ccn2C
HCID67854483

未命名化合物

收率 69.4%

PROCEDURE

实验过程

Using the procedure of Step C of Example 1, 43.7 g of the alcohol of Step B and 92.4 g of pyridinium dichromate were reacted to obtain 30.1 g of the expected product melting at 74° C. which was used as is for the following step.

WORKUP

后处理

  1. customwere reacted