HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cornforth reagent → (2-methoxyphenyl)-(1-methyl-1H-indol-4-yl) methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cornforth reagent | HCID 2724130 | — |
| Reactant | alpha-(2-methoxyphenyl)-1-methyl-1H-indol-4-methanol | HCID 19800111 | — |
| Product | (2-methoxyphenyl)-(1-methyl-1H-indol-4-yl) methanone | HCID 67854483 | 69.4% |
Reaction Steps
Using the procedure of Step C of Example 1, 43.7 g of the alcohol of Step B and 92.4 g of pyridinium dichromate were reacted to obtain 30.1 g of the expected product melting at 74° C. which was used as is for the following step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05086070 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-02a5032b27a54c558c2280e169b40d69 |
| Source note | uspto-grants-1992_02 |