HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 15623851, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | HCID 15623852 | HCID 15623852 | — |
| Product | HCID 15623851 | HCID 15623851 | — |
Reaction Steps
0.8 g (3.2 mmol) of 6-acetyl-3-amino-4-bromo-2-chloro-pyridine are dissolved in 5 ml of CHCl3, and 462 mg (3.42 mmol) of SO2Cl2, dissolved in 5 ml of CHCl3, are added. The mixture is stirred at room temperature for 30 minutes and then poured onto NaHCO3 solution and extracted with CH2Cl2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05086181 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-f5e6427b8a2c45c4994f63c98aaa1a10 |
| Source note | uspto-grants-1992_02 |