Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 14495798 | HCID 14495798 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 14495799 | HCID 14495799 | — |
Reaction Steps
3-Pentyl-1,2-difluorobenzene is metalated according to 1a) or 1b). A solution of 0.1 mol of iodine in 100 ml of diethyl ether is added slowly at -70° C. The mixture is subsequently stirred for a further hour at -70° C. and warmed to 0° C., and water is added to the solution. After washing with sodium hydrogen sulfite solution and dilute sodium hydroxide solution the mixture is worked up as customary.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05087764 |
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| Source dataset | uspto-grants-1992_02 |
|---|
| ORD ID | ord-e2970eb7b58e4f429d72665fc09f6d4f |
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| Source note | uspto-grants-1992_02 |
|---|
