HuagongsheHuagongshe Chemistry Print Report · For research reference only
hydroxylamine-O-sulfonic acid → 4-Ethoxy-2,3-difluorobenzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | hydroxylamine-O-sulfonic acid | HCID 76284 | — |
| Reactant | 4-Ethoxy-2,3-difluorobenzaldehyde | HCID 14495625 | — |
| Product | 4-Ethoxy-2,3-difluorobenzonitrile | HCID 14495626 | — |
Reaction Steps
4-Ethoxy-2,3-difluorobenzaldehyde (obtainable according to Example 7) is reacted with hydroxylamine -O-sulfonic acid according to J. Streith and C. Fizet, Helv. Chim. Acta 59, 2796 (1976), m.p.: 45° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05087764 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-f6aa0e6a36434f9b8a74e7822875e05e |
| Source note | uspto-grants-1992_02 |