HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54392015, compound → 1,2-Difluoro-3-propylbenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54392015 | HCID 54392015 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1,2-Difluoro-3-propylbenzene | HCID 14495703 | — |
Reaction Steps
Hydrogen is introduced at room temperature until saturation into a solution of 0.13 mol of 3-propenyl-1,2-difluorobenzene (obtainable according to Example 11) in 100 ml of THF containing 5 g of suspended Pd/C. Customary working up is carried out after stirring for 3 hours, b.p.30 : 72° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05087764 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-c3f34e8f179a421b85029ea005840929 |
| Source note | uspto-grants-1992_02 |