HCID 54392015, compound → 1,2-Difluoro-3-propylbenzene

HRID 1534270Notes

Reaction equation

HRID 1534270 reaction equation
[H][H].[CH:3]([C:6]1[C:7]([F:13])=[C:8]([F:12])[CH:9]=[CH:10][CH:11]=1)=[CH:4][CH3:5]>C1COCC1.[Pd]>[CH2:3]([C:6]1[C:7]([F:13])=[C:8]([F:12])[CH:9]=[CH:10][CH:11]=1)[CH2:4][CH3:5]

Participants

5

Reactant 2

HCID 54392015HCID 54392015, compoundHCID 178418361HCID 178418361, compound

Product 1

HCID 144957031,2-Difluoro-3-propylbenzene

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 8028TetrahydrofuranSolvent

Procedure

Hydrogen is introduced at room temperature until saturation into a solution of 0.13 mol of 3-propenyl-1,2-difluorobenzene (obtainable according to Example 11) in 100 ml of THF containing 5 g of suspended Pd/C. Customary working up is carried out after stirring for 3 hours, b.p.30 : 72° C.

Workup

  1. custom72° C.

Sources & evidence

ORD record
ord-c3f34e8f179a421b85029ea005840929
Source dataset
uspto-grants-1992_02
Patent number
US05087764

Reaction notes

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