2,3,3,4,4-Pentafluorocyclobutenyl isopropyl ether → 2,2,3,3-Tetrafluorocyclobutyl isopropyl ether
Reaction equation
[CH:1]([O:4][C:5]1[C:8]([F:10])([F:9])[C:7]([F:12])([F:11])[C:6]=1F)([CH3:3])[CH3:2]>CCOCC>[CH:1]([O:4][CH:5]1[CH2:6][C:7]([F:11])([F:12])[C:8]1([F:9])[F:10])([CH3:3])[CH3:2]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
280 g (1.39 mol) of 2,3,3,4,4-pentafluorocyclobutenyl isopropyl ether are hydrogenated in 1200 ml of ether as described in Example 5 and the mixture is worked up. 2,2,3,3-Tetrafluorocyclobutyl isopropyl ether is obtained in this way in a yield of 66% of theory.
Sources & evidence
- ORD record
- ord-1b26bf2bf099464e92fee7fbf534e827
- Source dataset
- uspto-grants-1992_02
- Patent number
- US05087775
Reaction notes
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