HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3,3,4,4-Pentafluorocyclobutenyl isopropyl ether → 2,2,3,3-Tetrafluorocyclobutyl isopropyl ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3,3,4,4-Pentafluorocyclobutenyl isopropyl ether | HCID 19911061 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2,2,3,3-Tetrafluorocyclobutyl isopropyl ether | HCID 19911062 | 66% |
Reaction Steps
280 g (1.39 mol) of 2,3,3,4,4-pentafluorocyclobutenyl isopropyl ether are hydrogenated in 1200 ml of ether as described in Example 5 and the mixture is worked up. 2,2,3,3-Tetrafluorocyclobutyl isopropyl ether is obtained in this way in a yield of 66% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05087775 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-1b26bf2bf099464e92fee7fbf534e827 |
| Source note | uspto-grants-1992_02 |