HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13448027, compound → HCID 53733853, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13448027 | HCID 13448027 | — |
| Reactant | HCID 19909486 | HCID 19909486 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 53733853 | HCID 53733853 | — |
Reaction Steps
Using the procedure of preparation B of Example 1, diethyl (formylamino)-(2-methyl-2-propenyl)-propanedioate in Step 2 was replaced by methyl 2-[(N-formylglycyl)-amino]-2-(2-propenyl)ethanoate to obtain the expected product with an Rf=0.2 in a methylene chloride/methanol (9:1) mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05089476 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-03d741cfec084fd4b7c31780efbd64d6 |
| Source note | uspto-grants-1992_02 |