2-(3,4-Dichlorophenyl)acetyl chloride → HCID 131717173, compound

Participants

Reaction Steps

g 1.4 (0.0077 moles) of 4-methyl-2-(1-pyrrolidinyl)methyl piperidine were reacted with g 2.1 (0.0093 moles) of 3,4-dichlorophenylacetyl chloride as described in Example 1. The oily residue so obtained (g 3.1) was chromatographed on 60 g of silica gel, eluting with CH2Cl2 containing increasing amounts of methanol (0.5 to 1.5%).

Provenance & Evidence