HuagongsheHuagongshe Chemistry Print Report · For research reference only
2H-Azepin-2-one, 3,3-dichlorohexahydro-5,5-dimethyl- → HCID 10607353, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2H-Azepin-2-one, 3,3-dichlorohexahydro-5,5-dimethyl- | HCID 10632227 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 10607353 | HCID 10607353 | 90% |
Reaction Steps
15.2 g (0.086 moles) of 3,3-dichloro-5,5-dimethyl-2-oxoperhydroazepine were dissolved in 900 ml of glacial acetic acid and shaked at 40 psi of hydrogen with 7 g of 10% Pd/C as in Description 14, to yield 13.6 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05089507 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-0b81547c0d3a4d7d989b21fb64f1242c |
| Source note | uspto-grants-1992_02 |