HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-alpha-methylbenzenemethanol → HCID 178450483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-alpha-methylbenzenemethanol | HCID 112058 | — |
| Reactant | Ethyl 2-butyryl-3-ethoxyacrylate | HCID 3359484 | — |
| Product | HCID 178450483 | HCID 178450483 | 96.8% |
Reaction Steps
2-(1-hydroxyethyl)aniline (30 g, 0.32 mol) and ethyl 2-butyryl-3-ethoxyacrylate (47.3 g, 0.22 mol) were heated together on a rotary evaporator (bath temperature 100° C.) for 1 hour to give ethyl 2-butyryl-3-(2-(1-hydroxyethyl)-phenylamino)acrylate as an oil (65 g, 96%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05089504 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-ffcd9c174d8a4962bf2dcdb8644d4fed |
| Source note | uspto-grants-1992_02 |