Lithium Hydroxide → HCID 178506973, compound

HRID 1534774Notes

Reaction equation

HRID 1534774 reaction equation
[OH-].[Li+:2].[SH:3]([O:6][C:7]([F:10])([F:9])[F:8])(=[O:5])=[O:4]>>[Li:2][S:3]([O:6][C:7]([F:10])([F:9])[F:8])(=[O:5])=[O:4]

Participants

3

Reactant 2

HCID 3939Lithium HydroxideHCID 178527253HCID 178527253, compound

Product 1

HCID 178506973HCID 178506973, compound

Procedure

To a lithium hydroxide (LiOH.2H2O, 4.20 g, 0.10 mol) aqueous solution, HSO3CF3 (15.01 g, 0.10 mol) was added dropwise. Water was evaporated from the resulting solution in a rotavapor, the residue was recrystallized in ethyl cyanide/toluene to yield LiSO3CF3. The LiSO3CF3 obtained was then dried under vaccum at 140° C. for 24 hr.

Workup

  1. customWater was evaporated from the resulting solution in a rotavapor
  2. customthe residue was recrystallized in ethyl cyanide/toluene

Sources & evidence

ORD record
ord-c6732fb68fb7459cba855d40f9d0ebff
Source dataset
uspto-grants-1992_02
Patent number
US05091274

Reaction notes

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