Hydrochloric Acid → HCID 19908400, compound

HRID 1534844Notes

Reaction equation

HRID 1534844 reaction equation
[O-:1][C:2]#[N:3].[K+].[C:5]([NH:10][NH2:11])([CH2:8][CH3:9])([CH3:7])[CH3:6].Cl>O>[C:5]([NH:10][NH:11][C:2]([NH2:3])=[O:1])([CH2:8][CH3:9])([CH3:7])[CH3:6]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 117546HCID 117546, compoundHCID 11378442Potassium cyanate

Product 1

HCID 19908400HCID 19908400, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

13.6 g of potassium cyanate are added to a mixture of 17 g of tert-pentylhydrazine and 30 ml of water cooled in an ice bath and 16.5 g of conc. hydrochloric acid are then added dropwise. The mixture is stirred at room temperature for 3 h and the solid is filtered off with suction, washed with water and dried in vacuo.

Workup

  1. temperaturecooled in an ice bath
  2. filtrationthe solid is filtered off with suction
  3. washwashed with water
  4. customdried in vacuo

Sources & evidence

ORD record
ord-4d8ee08daba343dfb7c4cd34613a8364
Source dataset
uspto-grants-1992_02
Patent number
US05091398

Reaction notes

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