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HRID1534845

反应详情

EQUATION

反应方程式

HRID 1534845 的结构方程式

REACTANTS

反应物

3
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CCC(C)(C)NNC(N)=O
HCID19908400

未命名化合物

结构：O=N[O-].[Na+]
HCID23668193

Sodium Nitrite

NNaO2

PRODUCTS

生成物

1
结构：CCC(C)(C)N(N=O)NC(N)=O
HCID19908401

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CO
溶剂HCID887

Methanol

CH4O

结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

1-tert-Pentyl semicarbazide (12 g) in a mixture of 50 ml of water and 25 ml of methanol is cooled in an ice bath and 5.6 g of sodium nitrite are added. Conc. hydrochloric acid is added dropwise to this solution until a pH of 4 to 5 is established.

WORKUP

后处理

  1. temperatureis cooled in an ice bath