HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Ethanedisulfenyl dichloride → HCID 21513871, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Ethanedisulfenyl dichloride | HCID 11816034 | — |
| Reactant | Carbamic acid, benzyldithio-, monosodium salt | HCID 23686905 | — |
| Product | HCID 21513871 | HCID 21513871 | — |
Reaction Steps
Bis-dithiocarbamates from primary amines are similarly prepared. For example, addition of 1,2-ethanedisulfenyl chloride solution to an aqueous solution of sodium benzyldithiocarbamate gives nearly a quantitative yield of 1,2-bis(N-benzylthiocarbamoyldithio)ethane, m.p. 105°-110°C, decom., NMR 7.3 singlet, 4.9 mult., 3.4 singlet and 3.15 singlet.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03979369 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-2de71e0804df452cac0a876e5978f145 |
| Source note | uspto-grants-1976_09 |