HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propenoic acid, 3-(3-methoxyphenyl)- → 3-(m-Methoxyphenyl)propionic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propenoic acid, 3-(3-methoxyphenyl)- | HCID 87155 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-(m-Methoxyphenyl)propionic acid | HCID 66336 | — |
Reaction Steps
Ten grams of m-methoxycinnamic acid in 100 ml. of ethanol is hydrogenated with 0.5 g. of pre-reduced 10% palladium-on-charcoal until the uptake of hydrogen ceases. The catalyst is removed by filtration and the filtrate evaporated to yield 3-(m-methoxyphenyl)propionic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03979458 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-2359c906a8ad4bd9882f11726ce20b51 |
| Source note | uspto-grants-1976_09 |