Dibenzylamine → HCID 22792493, compound

HRID 1576224Notes

Reaction equation

HRID 1576224 reaction equation
Br[CH:2]([CH3:16])[C:3]([C:5]1[CH:15]=[CH:14][C:8]([NH:9][S:10]([CH3:13])(=[O:12])=[O:11])=[CH:7][CH:6]=1)=[O:4].[CH2:17]([NH:24][CH2:25][C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1)[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>C(#N)C>[CH2:25]([N:24]([CH2:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[C@H:2]([C:3]([C:5]1[CH:15]=[CH:14][C:8]([NH:9][S:10]([CH3:13])(=[O:12])=[O:11])=[CH:7][CH:6]=1)=[O:4])[CH3:16])[C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1

Participants

4

Reactant 2

HCID 7656DibenzylamineHCID 13948301HCID 13948301, compound

Product 1

HCID 22792493HCID 22792493, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

Reaction of 4'-(2-bromopropionyl)methanesulfonanilide with 2 molar equivalents of dibenzylamine in acetonitrile provides 4'-(N,N-DIBENZYLALANYL)METHANESULFONANILIDE purified as the hydrochloride, m.p. 216.0°-218.0°C. (dec.).

Sources & evidence

ORD record
ord-55b34136d1c64ef1aabcffaf8d88e6ae
Source dataset
uspto-grants-1976_09
Patent number
US03979514

Reaction notes

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