Azobisisobutyronitrile → Acrylamido methyl-4-hydroxy benzophenone stearyl methacrylate

HRID 1576292Notes

Reaction equation

[Pb].[N].[C:3]([NH:7][CH2:8][C:9]1[CH:22]=[C:21]([OH:23])[CH:20]=[CH:19][C:10]=1[C:11]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)=[O:12])([CH:5]=[CH2:6])=[O:4].[C:24]([O:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH3:47])(=[O:28])[C:25]([CH3:27])=[CH2:26].N(C(C)(C)C#N)=NC(C)(C)C#N>CC(C)=O>[C:3]([NH:7][CH2:8][C:9]1[CH:22]=[C:21]([OH:23])[CH:20]=[CH:19][C:10]=1[C:11]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)=[O:12])(=[O:4])[CH:5]=[CH2:6].[C:24]([O:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH3:47])(=[O:28])[C:25]([CH3:27])=[CH2:26]

Participants

Conditions

Temperature: 80 °C

Procedure

Into a 50 ml flask provided with a condenser, a nitrogen lead in tube and an agitator, there are introduced 1g of acrylamino methyl 4-hydroxy benzophenone, 1.5g of stearyl methacrylate and 0.25g of azobis-isobutyronitrile in solution in 5 ml of acetone. The resulting mixture is heated for 8 hours at 80°C.

Workup

customInto a 50 ml flask provided with a condenser

Sources & evidence

ORD record: ord-90da6adbff424421a5e2a77a024158bb
Source dataset: uspto-grants-1976_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03980617

Reaction notes

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