HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 54347004, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | HCID 21512627 | HCID 21512627 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54347004 | HCID 54347004 | — |
Reaction Steps
A solution of 105.5 g 3-(4'-fluoro-4-biphenylyl)-3-hydroxybutyric acid and 5.3 g p-toluenesulfonic acid in 1500 ml of toluene is heated for 2,5 hours and worked up in the usual manner to give 3-(4'-fluoro-4-biphenylyl)-2-butenoic acid, m.p. 58° - 60°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03980795 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-288e20695f7e45bc87e2cb0298d33a09 |
| Source note | uspto-grants-1976_09 |