HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloride → HCID 86733985, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloride | HCID 312 | — |
| Reactant | 3-Chloropropionic acid | HCID 7899 | — |
| Reactant | N-Phenyl-1,2,3,4-tetrahydronaphthalen-2-amine | HCID 12403842 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 86733985 | HCID 86733985 | — |
Reaction Steps
0.1 mol of 2-phenylamino-1,2,3,4-tetrahydronaphthalene, 0.15 mol of the chloride of β-chloropropionic acid and 25 ml of benzene are refluxed during 4.5 hours. The solvent and the reagent excess are then removed. The residue is recrystallized from petroleum ether. M.P. 78°-81°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03981872 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-483cef0b4dcf4c9987573e29393cad21 |
| Source note | uspto-grants-1976_09 |