Chloride → HCID 86733985, compound

HRID 1576502Notes

Reaction equation

HRID 1576502 reaction equation
[C:1]1([NH:7][CH:8]2[CH2:17][CH2:16][C:15]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[CH2:9]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Cl-].[Cl:19][CH2:20][CH2:21][C:22](O)=[O:23]>C1C=CC=CC=1>[C:1]1([N:7]([CH:8]2[C:9]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[CH2:15][CH2:16][CH2:17]2)[C:22](=[O:23])[CH2:21][CH2:20][Cl:19])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

5

Reactant 3

HCID 312ChlorideHCID 78993-Chloropropionic acidHCID 12403842N-Phenyl-1,2,3,4-tetrahydronaphthalen-2-amine

Product 1

HCID 86733985HCID 86733985, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

0.1 mol of 2-phenylamino-1,2,3,4-tetrahydronaphthalene, 0.15 mol of the chloride of β-chloropropionic acid and 25 ml of benzene are refluxed during 4.5 hours. The solvent and the reagent excess are then removed. The residue is recrystallized from petroleum ether. M.P. 78°-81°C.

Workup

  1. customThe solvent and the reagent excess are then removed
  2. customThe residue is recrystallized from petroleum ether

Sources & evidence

ORD record
ord-483cef0b4dcf4c9987573e29393cad21
Source dataset
uspto-grants-1976_09
Patent number
US03981872

Reaction notes

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