HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 13289787, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-(6-Carboxyoctyl)-2-cyclopentenone | HCID 21767816 | — |
| Product | HCID 13289787 | HCID 13289787 | — |
Reaction Steps
Treatment of 2-(6-carboxyoctyl)-2-cyclopentone (Example 131) with thionyl chloride and then treatment of the acid chloride with ethanol in the manner described in Example 456 gives an amber oil. The oil is placed on a magnesia-silica gel column and eluted with 3:1 benzene:ether. The solvent is removed and the residue is distilled, b.p. 122°C. (0.06 mm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03981868 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-9282ce4a2e184f19b8d3adbde24cb7db |
| Source note | uspto-grants-1976_09 |