HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 21511444, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Hydride | HCID 166653 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 21511439 | HCID 21511439 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 21511444 | HCID 21511444 | — |
Reaction Steps
Ethyl 2-[4-(4-fluorophenoxy)phenyl]propionate (1.3 g.) in dry ether (5 ml.) was added dropwise to lithium aluminium hydride (200 mg.) in dry ether (5 ml.). After refluxing for 1 hour the excess hydride was decomposed with dilute sulfuric acid, and the ether layer was distilled to give 2-[4-(4-fluorophenoxy)phenyl]propanol, b.p. 151°-152°C./0.6 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03981905 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-16373e5b8c2e42a092af6b67a631f7b0 |
| Source note | uspto-grants-1976_09 |