HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → AE-848/34436008
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 21511588 | HCID 21511588 | — |
| Solvent | Water | HCID 962 | — |
| Product | AE-848/34436008 | HCID 3139336 | 84% |
Reaction Steps
N-(2,2,6,6-Tetramethyl-4-piperidyl)-3,5-dinitrobenzamide hydrochloride (18.5 g.) is dissolved in water (350 ml.) and the pH adjusted to 11 with 1.0N NaOH. A cream colored precipitate forms and is collected by filtration, washed with water and dried (14.1 g., m.p. 220°-222°, 84% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03982006 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-c43a991c4e93418fa9ef70db2203bc21 |
| Source note | uspto-grants-1976_09 |