HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 54350597, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | Thiosemicarbazide | HCID 2723789 | — |
| Reactant | HCID 54466296 | HCID 54466296 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54350597 | HCID 54350597 | — |
Reaction Steps
1.0 g of 2-(4-bromophenyl)-3-(5-nitro-2-furyl) acrolein and 0.31 g of thiosemicarbazide are heated at reflux for 30 minutes in 25 cc of methanol with 0.3 g of glacial acetic acid and 1.0 g of sodium acetate. Upon cooling, the title compound is obtained as yellow brown crystals having a M.P. of 230°-237°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03982007 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-4d7f4e03155a4c67927bf6c6c8d5a8a8 |
| Source note | uspto-grants-1976_09 |