Hydrochloric Acid → HCID 68146413, compound

HRID 1576668Notes

Reaction equation

HRID 1576668 reaction equation
Cl.[C:2]([O:5][C:6]1([C:19]2[CH:24]=[CH:23][C:22]3[O:25][CH2:26][O:27][C:21]=3[CH:20]=2)[CH2:11][CH2:10][N:9](CC2C=CC=CC=2)[CH2:8][CH2:7]1)(=[O:4])[CH3:3].Cl>>[C:2]([O:5][C:6]1([C:19]2[CH:24]=[CH:23][C:22]3[O:25][CH2:26][O:27][C:21]=3[CH:20]=2)[CH2:11][CH2:10][N:9]([CH2:8][CH2:7][CH2:6][C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[CH2:8][CH2:7]1)(=[O:4])[CH3:3]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 68146319HCID 68146319, compound

Product 1

HCID 68146413HCID 68146413, compound

Procedure

4-Acetoxy-4-(3.4-methylene dioxy phenyl)-piperidine hydrochloride (M.P. 167° - 168°C) is obtained in analogous manner to that described in Example 1d from 4-Acetoxy-1-benzyl-4-(3.4-methylene dioxy phenyl)-piperidine hydrochloride with no free hydrochloric acid and at a temperature of 40° - 50°C.

Sources & evidence

ORD record
ord-516fbf5ce48541ebad48871dbf8017c6
Source dataset
uspto-grants-1976_09
Patent number
US03982001

Reaction notes

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