HuagongsheHuagongshe Chemistry Print Report · For research reference only
Succinimide → HCID 22764837, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Succinimide | HCID 11439 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Phenyl chloroformate | HCID 15891 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 22764837 | HCID 22764837 | — |
Reaction Steps
To 50 millimolses of phenylchloroformate in 25 ml of ether are added 16.7 ml of a 3M potassium hydroxide solution containing 50 millimoles of predissolved succinimide. The system is then stirred for about 1 hour, additional ether added and then restirred for about 1 hour. The insolubles formed are removed by filtering. Thereafter, the crude product is recrystallized from butanol saturated with water to give the desired product, melting point 132° - 133.5°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03982891 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-d4de682981ae4acebb8f04f81735ddec |
| Source note | uspto-grants-1976_09 |