HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 131710455, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | HCID 131710456 | HCID 131710456 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 131710455 | HCID 131710455 | — |
Reaction Steps
3-Chloro-5-[3-(4-methyl-1-piperazinyl)propyl]-2-phenyl-1,5-benzothiazepin-4(5H)-one, hydrochloride (prepared as described in Example 1) is treated with one equivalent of hydrogen peroxide in dilute acetic acid, and allowed to stand for about 16 hours. Solvent removal yields the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03983106 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-75bb68ad271f41cca3de9259a9eb0496 |
| Source note | uspto-grants-1976_09 |