HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 21509629, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 13428332 | HCID 13428332 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21509629 | HCID 21509629 | — |
Reaction Steps
A solution of 10 parts of 1-methyl-3-isopropyl-6-methylthio-s-triazine-2,4(1H,3H)-dione in 100 parts of tetrahydrofuran at 0° is saturated with dimethylamine. The reaction is allowed to warm to room temperature and stand overnight. The solvent is evaporated and the residue triturated with ether to afford 9 parts of 1-methyl-3-isopropyl-6-dimethylamino-s-triazine-2,4(1H,3H)-dione, m.p. 104°-106°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03983116 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-713db524186c42058b681ed2265110a7 |
| Source note | uspto-grants-1976_09 |