Dimethylamine → HCID 21509629, compound

HRID 1576765Notes

Reaction equation

HRID 1576765 reaction equation
[CH3:1][N:2]1[C:7](SC)=[N:6][C:5](=[O:10])[N:4]([CH:11]([CH3:13])[CH3:12])[C:3]1=[O:14].[CH3:15][NH:16][CH3:17]>O1CCCC1>[CH3:1][N:2]1[C:7]([N:16]([CH3:17])[CH3:15])=[N:6][C:5](=[O:10])[N:4]([CH:11]([CH3:13])[CH3:12])[C:3]1=[O:14]

Participants

4

Reactant 2

HCID 674DimethylamineHCID 13428332HCID 13428332, compound

Product 1

HCID 21509629HCID 21509629, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

A solution of 10 parts of 1-methyl-3-isopropyl-6-methylthio-s-triazine-2,4(1H,3H)-dione in 100 parts of tetrahydrofuran at 0° is saturated with dimethylamine. The reaction is allowed to warm to room temperature and stand overnight. The solvent is evaporated and the residue triturated with ether to afford 9 parts of 1-methyl-3-isopropyl-6-dimethylamino-s-triazine-2,4(1H,3H)-dione, m.p. 104°-106°.

Workup

  1. customat 0°
  2. customThe solvent is evaporated
  3. customthe residue triturated with ether

Sources & evidence

ORD record
ord-713db524186c42058b681ed2265110a7
Source dataset
uspto-grants-1976_09
Patent number
US03983116

Reaction notes

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