Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → 2-Phenylmorpholine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | alpha-[[(2-Hydroxyethyl)amino]methyl]benzyl alcohol | HCID 107278 | — |
| 용매 | Hydrochloric Acid | HCID 313 | — |
| 생성물 | 2-Phenylmorpholine | HCID 91101 | — |
반응 단계
N-(2'-hydroxy-2'-phenylethyl)-ethanolamine (5.3 g.) was dissolved in 6N hydrochloric acid (100 ml.) and the solution heated at 110° for 4 hours. The mixture was basified with sodium hydroxide solution and extracted into ether. The extract was washed with water, dried over anhydrous sodium sulphate and evaporated to give a crude sample of title compound (Ig.) as an orange oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03983111 |
| 출처 데이터셋 | uspto-grants-1976_09 |
| ORD ID | ord-bf144086edc844319fcbfdcb38de581a |
| 출처 메모 | uspto-grants-1976_09 |