HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Benzyloxybenzoylchloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-(Benzyloxy)benzoic acid | HCID 73880 | — |
| Product | 4-Benzyloxybenzoylchloride | HCID 3766410 | — |
Reaction Steps
4-Carboxyphenoxy phenyl methane (20g) was converted to the acid chloride by heating under reflux with thionyl chloride for 1hr. Excess thionyl chloride was removed by distillation to yield 4-chlorocarbonylphenoxy phenyl methane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03983164 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-0fdab01ee6eb4d6da66ec148a21483be |
| Source note | uspto-grants-1976_09 |