HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 12398505, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | O-Xylene | HCID 7237 | — |
| Reactant | 4-Benzyloxybenzoylchloride | HCID 3766410 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 12398505 | HCID 12398505 | — |
Reaction Steps
A mixture of 4-chlorocarbonylphenoxy phenyl methane (12.3g.; 0.05 mole), propan-2-ol (3.6g.; 0.6 mole), pyridine (5g) and xylene (50ml) were boiled under reflux for 18hr. The cooled mixture was poured into water and extracted with dichloromethane. The organic extract was washed well with water and dried (anhyd. MgSO4), filtration and evaporation yielded 4-isopropoxycarbonylphenoxy phenyl methane, m.p. 62°-3°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03983164 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-fdb3f11995c74d6388043edfd4481038 |
| Source note | uspto-grants-1976_09 |