HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitrosyl chloride → HCID 3303868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitrosyl chloride | HCID 17601 | — |
| Reactant | HCID 19475 | HCID 19475 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 3303868 | HCID 3303868 | 35.4% |
Reaction Steps
By the method of Example I-B, 67.6 g of 4-methylbenzaldoxime in 600 ml of ether was treated with 39.3 g of nitrosyl chloride. After removal of the ether, the product was recrystallized twice from hexane to give 30 g of 4-methylbenzohydroximoyl chloride, m.p. 70°-73°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03983246 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-aef5f21b8b30495c9670aac3a9091895 |
| Source note | uspto-grants-1976_09 |