HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 20530897, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 19884404 | HCID 19884404 | — |
| Product | HCID 20530897 | HCID 20530897 | 97.1% |
Reaction Steps
11 g of thionyl chloride was added to 14.5 g (0.046 mol) of the 3-bromo-4-n-heptyloxybenzoic acid prepared in Step II and was gently refluxed for two hours. Excess thionyl chloride was removed by distillation or vacuum distillation to yield 14.9 g of 3-bromo-4-n-heptyloxybenzoyl chloride. The yield was calculated to be 96.8%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04287085 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-423209115d8e4b80806c148bbf759eaf |
| Source note | uspto-grants-1981_09 |