HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl isothiocyanate → N-[2-[[5-(Dimethylaminomethyl)-4-methyl-2-furanylmethyl]thio]ethyl]-N'-methylthiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl isothiocyanate | HCID 11167 | — |
| Reactant | 2-[(5-Dimethylaminomethyl-4-methyl-2-furyl)methylthio]ethylamine | HCID 13125117 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N-[2-[[5-(Dimethylaminomethyl)-4-methyl-2-furanylmethyl]thio]ethyl]-N'-methylthiourea | HCID 20570933 | — |
Reaction Steps
A solution of 5-[[2-(amino)ethyl]thio]methyl-N,N,3-trimethyl-2-furanmethanamine (0.5 g) and methylisothiocyanate (0.15 ml) in dry acetonitrile was stirred for 24 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04288443 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-4bdc598375c547bcb0bfd9b905d88798 |
| Source note | uspto-grants-1981_09 |