HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylthio-1-methylamino-2-nitroethylene → HCID 131712379, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylthio-1-methylamino-2-nitroethylene | HCID 123549 | — |
| Reactant | HCID 20570927 | HCID 20570927 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 131712379 | HCID 131712379 | 71.7% |
Reaction Steps
A mixture of 5-[[2-(amino)ethyl]thio]methyl-N-methyl-3-phenyl-2-furanmethanamine (0.45 g) and N-methyl-1-(methylthio)-2-nitroethenamine (0.24 g) was stirred in water (5 ml) for 24 hours. The solvent was removed in vacuo and the residue purified by column chromatography (Silica/methanol) affording the title compound (0.3 g) as an amber glass.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04288443 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-7f94373ec7174466ae4671f59ef3195b |
| Source note | uspto-grants-1981_09 |