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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1577512Generated: October 30, 2026

1-Methylthio-1-methylamino-2-nitroethylene → HCID 131712379, compound

https://huagongshe.com/reaction/1577512

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Methylthio-1-methylamino-2-nitroethyleneHCID 123549—
ReactantHCID 20570927HCID 20570927—
SolventWaterHCID 962—
ProductHCID 131712379HCID 13171237971.7%

Reaction Steps

A mixture of 5-[[2-(amino)ethyl]thio]methyl-N-methyl-3-phenyl-2-furanmethanamine (0.45 g) and N-methyl-1-(methylthio)-2-nitroethenamine (0.24 g) was stirred in water (5 ml) for 24 hours. The solvent was removed in vacuo and the residue purified by column chromatography (Silica/methanol) affording the title compound (0.3 g) as an amber glass.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04288443
Source datasetuspto-grants-1981_09
ORD IDord-7f94373ec7174466ae4671f59ef3195b
Source noteuspto-grants-1981_09